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A guide to Fabry-Perot polymer film ultrasound detection

Principles of operation | Sensitivity | Linearity | Frequency response | Effective element size


Principles of operation

Figure 1(a) shows a schematic of a Fabry-Perot polymer film ultrasound transducer. A discrete polymer film such as PET (polyethyene terephthalate) or one that is deposited on to a substrate such as Parylene can be used as the sensing element. The thickness of the polymer film depends up the bandwidth required and backing configuration but is typically of the order of 25-50µm for bandwidths in the tens of MHz range. The “mirrors” of the interferometer can be formed by depositing metallic or dielectric reflective coatings or for certain applications [1,2] left uncoated with the refractive index mismatch between the film and surrounding media providing the necessary Fresnel reflections. The transduction mechanism [3] comprises two processes. Firstly, assuming the elastic limits of the polymer sensing film are not exceeded, external acoustic pressure is linearly converted to a change in the optical thickness of the film (fig 1(a)). Secondly, the resulting optical phase shift is converted to an intensity (figure 1(b)) modulation through the intensity-phase transfer function of the interferometer. The latter is not strictly linear although by setting the phase bias appropriately (see figure 2(b)) by tuning the laser wavelength, small phase shifts can be detected with acceptable linearity.

Figure 1 (a) Fabry-Perot polymer film ultrasound sensor and (b) low finesse Fabry-Perot interferometer transfer function.

Note that figure 1(b) shows the raised cosine transfer function characteristic of a two beam interferometer. In a F-P cavity, this occurs when the reflectivities of the cavity mirrors are small (<10%). In this case the contribution of multiple reflections to the reflected fringe system can be neglected and the interferometer becomes one of low finesse. Whilst higher sensitivity can be achieved using high reflectivity low absorption dielectric mirrors to create a high finesse F-P cavity, there are several important practical advantages to the low finesse configuration. It offers reasonable detection sensitivity, comparable to PVDF transducers and a useful linear phase range with the detection of phase shifts up to 0.8 rad achievable with a linearity of better than 10%. An optimum fringe visibility close to unity can be achieved with a relatively wide range mirror reflectivities reducing the requirements of the optical coating process. Furthermore, the wavelength tuning range and stability requirements for the laser source are relatively relaxed compared to those for a high finesse cavity.

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Sensitivity

To formalise the description of sensitivity it is helpful to define figures of merit for each transduction process [3]. The phase sensitivity Is represents the slope efficiency of the conversion of optical phase df to intensity output dIR and is defined as the optical power modulation per unit phase shift (mW/rad) at the phase bias fo (figure 1b).

                  (1)

Thus Is is dependent upon the incident laser power and the reflectivity and absorbance characteristics of the reflective coatings that form the mirrors of the interferometer. With knowledge of the detector noise floor, Is can be used to determine the phase resolution of the interferometer - mrad phase noise floors over a 25MHz measurement bandwidth with low finesse cavities have been reported [3,4].

The acoustic phase sensitivity As represents the conversion of external acoustic pressure to an optical phase shift. It is defined as magnitude of the optical phase shift produced per unit acoustic pressure (rad/MPa). It is thus a measure of the acoustically-induced change in optical thickness of the sensing film - the change in both physical thickness and refractive index and is dependent on the elastic and photoelastic properties of the cavity. It is given by

            (2)

where n is the refractive index, l is the thickness of the film, l the laser wavelength, E the Young's modulus, p the photoelastic constant, s  Poisson's ratio. k is the acoustic wavenumber, k=2p/la where la is the acoustic wavelength.

PI(k) is a frequency-dependent modifying term (discussed further in the frequency response section) representing the net stress integrated across the thickness of the sensing film and is dependent upon the acoustic properties of the film, the backing material and the surrounding media (usually water). In the low frequency limit where la >> l, assuming the acoustic impedance mismatch between the sensing film and the surrounding fluid is small, |P(k)| is dominated by the acoustic properties of the backing material. At low frequencies, |P(k)| = 0 for a compliant backing such as air, |P(k)| ~ 1 for a backing of similar acoustic impedance such as water or a polymer and |P(k)| ~ 2 for a rigid backing such as glass. In this paper, the low frequency limit is implied when discussing acoustic phase sensitivity for a particular backing configuration.

The acoustic phase sensitivity enables (with knowledge of the form of the interferometer transfer function (ITF)) the acoustic pressure range over which the sensor is linear to be estimated and comparisons to be made between the intrinsic sensitivity of different sensing film materials, thicknesses and backing configurations. Typical values for As for 50µm thick water-backed polymer films at 850nm are 0.1 rad/MPa for PET [3] and 0.075rad/MPa for Parylene [4]. For a low finesse cavity, this gives an upper limit of linear (<10%) detection of 10MPa and a dynamic range of 60dB.

The product of Is and As gives the overall sensitivity. In principle, this could be optimised through As by selecting a polymer with appropriately high values of p and E. In practice, this is problematic due to the paucity of data available in the literature for these parameters at ultrasonic frequencies. Additionally, the selection of the polymer film tends to be dominated more by considerations of uniformity of thickness, surface finish and optical clarity than its mechanical/elastic properties. To optimise sensitivity it is more fruitful to consider the detector noise floor and the characteristics of the interferometer transfer function.

With a wideband (tens of MHz) silicon photodiode-transimpedance amplifier detector configuration, the output system noise tends to be dominated by a combination of the amplifier input noise voltage and the shot noise due to the photocurrent arising from the (large) dc interferometer output level IR. 0.05µW noise-equivalent powers are typical although there is the potential for some improvement on this by reducing the amplifier input noise voltage. Greater scope for improving sensitivity lies in optimising the interferometer transfer function. For a low finesse configuration, it is desirable to design for a fringe visibility of unity and operate at a laser power such that the output dc level IR is just below the saturation threshold of the detector. 10kPa noise equivalent pressures (over a 25MHz measurement bandwidth), comparable to PVDF transducers are readily achieved with such a configuration. To improve upon this requires the design of a high finesse cavity to “sharpen” the transfer function. At least an order of magnitude increase in sensitivity should be possible albeit with a reduced upper limit of linear detection. Additionally, an increased wavelength tuning range is required in order to avoid the 2p radians of "dead space" between the resonant peaks of ITF where sensitivity is zero. Higher wavelength stability is also necessary to hold the system at the optimum phase bias.

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Linearity

Assuming the elastic limits of the polymer film are not exceeded, the upper limit of linear acoustic detection is determined by the characteristics of the interferometer transfer function. The analysis is simplest for a low finesse interferometer which has a characteristic raised sinusoidal transfer function. At the quadrature point, phase shifts up to 0.5rad can be resolved with a linearity of better than 5% and using the acoustic phase sensitivity this can be converted to acoustic pressure. So for a 25µm rigid backed Parylene film with an acoustic phase sensitivity of 0.075rad/MPa, linear operation to 7MPa can be expected as shown in figure 2 [4]. If a reduced linearity of 10% can be tolerated, in upper limit of 11MPa and a dynamic range of 60dB will be obtained.

Figure 2 Linearity of an optical fibre hydrophone employing a 25 µm thick Parylene sensing film (rigid-backed) [4]. Predicted curve is based upon measured acoustic phase sensitivity of 0.075 rad/MPa and the assumption of a low finesse Fabry Perot sensing cavity. The dotted vertical lines shows the acoustic pressure at which the sensor nonlinearity becomes 5% and 10%.

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Frequency response

For a sensing film of sufficiently large lateral dimensions, radial resonance modes and the effects of acoustic diffraction at the boundaries of the film can be neglected. The sensor is then said to operate in thickness mode. The frequency response Pl(k) depends upon the spatial variation of acoustic pressure PT due to the incident acoustic wave and its reflection within the film arising from the acoustic impedance mismatch at its boundaries. Pl(k) is obtained by evaluating the mean distribution of stress across the thickness l of the film as a function of frequency [3].

            (3)

where k is the acoustic wavenumber. The thickness of the sensing film in relation to the acoustic wavelength determines the bandwidth. The acoustic impedance mismatches at the boundaries of the film, on one side due to the backing, on the other due to water determines the uniformity of response. In general, polymer films have an acoustic impedance close to water and the uniform broadband response characteristics of a low Q system can be expected.

Figure 3 Acoustic reflections within sensing film.

Figure 4 shows the experimentally measured frequency response of three physically useful configurations [3]. In each case 50 µm thick PET sensing films were used. The water backed configuration shows the small l/2 thickness mode resonance (at ~20MHz) characteristic of a water backed polymer film - a similar response can be observed with PVDF membrane hydrophones. For the glass backed sensing film, which approximates to a rigid backed configuration, ( |P(k)| = 2) and the bandwidth is reduced by a factor of 2 with a l/4 resonance at approximately 9 MHz. The resonance is at a slightly lower frequency than it should be due to bandlimiting effect of the adhesive layer (~1.5 µm) between the sensing film and glass backing. In the PMMA-backed configuration, the acoustic impedance of the PET sensing film, adhesive layer and PMMA backing are very similar (~3 x 106 kg/m2 s). Thus there is no resonance and the response rolls off with increasing frequency.

Figure 4 Experimentally measured frequency responses of three different backing configuration using 50µm PET sensing film [3]. The continuous lines show the predicted response calculated using equation 3.

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Effective element size

The effective element size is a measure of the acoustic aperture of a receiver. Its effect on lateral spatial resolution makes it a key parameter in an ultrasonic measurement and imaging system. It is of particular importance for an ultrasound field characterisation tool such as a hydrophone or in phased array systems where the requirement is for each element to have a near isotropic directional response requiring the element size to be small in relation to the acoustic wavelength. To a first approximation, the element size of the FP polymer film sensing concept is defined by the dimensions of the optical field addressing the film. Thus, in principal, element sizes down to the optical diffraction limit of a few microns are feasible offering the prospect of an omni-directional response at acoustic frequencies as high as 50MHz. This can be achieved without compromising sensitivity as, unlike piezoelectric transducers, sensitivity is independent of element size for a given optical intensity.

Clearly there will be a limit to the assumption that the active area is defined only by the region that is optically addressed. Acoustically-induced thickness deformations outside the optically defined area of an “element” will, to some extent, contribute to its output increasing the acoustic aperture. This effect can be assessed by measuring the directional response of the element as a function of acoustic frequency. By fitting the first order Bessel function of the angular response of a circular plane piston in a rigid baffle to the experimental data, the effective radii at each frequency can be determined. This has been studied in a previous paper [4] by illuminating a polymer sensing film with the output of a 6µm core diameter single mode optical fibre. Directivity measurements at several frequencies are shown in figure 5(a) illustrating low directional sensitivity to 10 MHz. The corresponding effective radii at 1 MHz intervals to 10 MHz are shown in figure 5(b). In common with piezoelectric PVDF receivers, the effective radii falls off with frequency. This is thought to be due to the apodised response of the sensor arising from the Gaussian profile of the output of the single mode optical fibre. Beyond 10 MHz, where the effective radii (not shown in fig 5(b)) would be expected to level out a value close to optically defined element size, the effects of acoustic diffraction around the tip of the fibre were found to distort the directivity plots making it impossible to recover the effective radius. Thus it is difficult to say categorically what eventual minimum effective radius would be. However, from the measurements below 10 MHz the effective radius is (at worst) estimated at 35 µm and is quite possibly significantly lower.

Figure 5 (a) Directional response of FP polymer film transducer illuminated with the output of a 6µm core single mode optical fibre (b) Effective radius as a function of frequency. [4]

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